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Read online book Interpretation of NMR Data by Neil E. Jacobsen DJV, DOC, MOBI


The book starts at the simplest level, with little or nodiscussion of NMR theory or physics, and focuses entirely on alarge number of examples of NMR data. Through these examples,the principles of the relationship between chemical structure andthe NMR spectrum are developed in a logical, step-by-stepfashion. After each new concept is introduced there arenumerous problems to illustrate the concept. While startingwith the simplest concepts and examples, the book does progress tocomplex topics not usually covered in NMR books such as: complex splitting patterns, stereochemistry in rigid molecules,prediction of J coupling values, effects of chirality, stericcrowding effects, and resonance structure analysis for predictionof chemical shifts. Advanced topics include all of the commontwo-dimensional experiments (COSY, NOESY, TOCSY, HSQC, HMBC)covered strictly from the point of view of data interpretation,with many examples and problems. These are valuable tools for theserious user of NMR data in research., Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings

Interpretation of NMR Data in EPUB, DOC, FB2

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